Identification—
Digest about 2 g with 5 mL of nitric acid over gentle heat for 1 hour, dilute with water to about 50 mL, and filter: the solution responds to
Identification test
A under
Selenium Sulfide, when tested as directed, beginning with “to 10 mL of the filtrate add 5 mL of water.”
Assay—
Place a portion of well-mixed Lotion, equivalent to about 100 mg of selenium sulfide and accurately weighed, in a suitable flask. Cautiously digest with 25 mL of fuming nitric acid over gentle heat for 2 hours, and proceed as directed in the
Assay under
Selenium Sulfide, beginning with “Cool, transfer the solution to a 250-mL volumetric flask.” Each mL of 0.05 N sodium thiosulfate is equivalent to 1.789 mg of SeS
2. Where the Lotion is labeled in terms of percentage (w/v) or of the amount of SeS
2 in a given volume of Lotion, determine the density of the Lotion as follows: Using a tared, 100-mL volumetric flask, weigh 100 mL of Lotion that previously has been shaken to ensure homogeneity, allowed to stand until the entrapped air rises, and finally inverted carefully just prior to transfer to the volumetric flask. From the observed weight of 100 mL of the Lotion, calculate the quantity of SeS
2 in each 100 mL.
791
:
between 2.0 and 6.0.